bis(4-cobaltoceniumyl-1-ferrocenyl-3-methyl-1,2,3-triazolylidene)gold(i) hexafluoridophosphate–trifluoromethanesulfonate (1.2/1.8)

bis(4-kobaltosenyumil-1-ferrosenil-3-metil-1,2,3-triazoliliden)altın(I) heksafloridofosfat–triflorometansülfonat (1,2/1,8)

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ID: 193160
2018
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Abstract
The title compound, [AuCo2Fe2(C5H5)4(C13H11N3)2](PF6)1.2(CF3SO3)1.8, was synthesized by deprotonation of 4-cobaltoceniumyl-1-ferrocenyl-3-methyl-1,2,3-triazolium hexafluoridophosphate trifluoromethanesulfonate with thallium ethoxide, followed by transmetalation with chlorido(triphenylphosphine)gold(I), crystallizing as orange prisms. It is a unique example of a homoleptic dimetallocenyl-substituted triazolylidene complex.
Başlık bileşiği olan [AuCo2Fe2(C5H5)4(C13H11N3)2](PF6)1.2(CF3SO3)1.8; 4-kobaltosenyumil-1-ferrosenil-3-metil-1,2,3-triazolyum heksafloridofosfat triflorometansülfonatın talyum etoksit ile deprotonasyonu ve ardından klorido(trifenilfosfin)altın(I) ile transmetalasyonu yoluyla sentezlenmiş olup turuncu prizmalar hâlinde kristallenmiştir. Bu bileşik, homoleptik dimetalosenil sübstitüeli bir triazoliliden kompleksinin benzersiz bir örneğidir.
Reference Key
vanicek2018iucrdatabis(4-cobaltoceniumyl-1-ferrocenyl-3-methyl-1,2,3-triazolylidene)gold(i) Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors ;Stefan Vanicek;Klaus Wurst;Holger Kopacka;Benno Bildstein
Journal lecture notes in civil engineering
Year 2018
DOI
10.1107/S2414314618006235
URL
http://scripts.iucr.org/cgi-bin/paper?S2414314618006235
Keywords
gold crystal structurecrystallography

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