estudo espectroscópico de compósito obtido da reação no estado sólido entre um complexo mononuclear de vanádio(iv) e caulinita
Clicks: 110
ID: 189376
2012
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Abstract
The use of probes, such as paramagnetic species diluted in diamagnetic materials in EPR spectroscopy, and mathematical tools such, as the Kubelka-Munk function in DRUV-VIS spectroscopy are strategies in the analysis of complex mixtures of solid materials. The results obtained here show that the solid state reaction between the complex, [VO(acac)(BMIMAPY)] [ClO4], BMIMAPY = [(bis(1-methylimidazole-2-yl)methyl)(2-(pyridyl-2-yl)ethyl) amine] and acac = acetilacetonate, with kaolinite turns possible to obtain anisotropic EPR spectrum of the complex with a reasonable level of resolution. The study by DRUV-VIS using the method of second derivative mode of the Kubelka-Munk function revealed new complex structural arrangements, a solid hitherto unknown.
| Reference Key |
rezende2012qumicaestudo
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|---|---|
| Authors | ;Edivaltris I. P. De Rezende;Antonio S. Mangrich;Ana P. Mangoni;Marciela Scarpellini;Annelise Casellato;Tatiana L. Fernández |
| Journal | greece and rome |
| Year | 2012 |
| DOI |
10.1590/S0100-40422012000200005
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| URL | |
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