determination of fipronil in bovine plasma by solid-phase extraction and liquid chromatography with ultraviolet detection
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ID: 184923
2012
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Abstract
A fast and efficient method has been developed and validated for the determination of fipronil in bovine plasma. Samples were subjected to solid-phase extraction (SPE) followed by reversed phase liquid chromatography (LC) separation, using acetonitrile/water (60:40 v/v) as the mobile phase with a flow rate of 1.0 mL/min and ultraviolet (UV) detection at 210 nm. Ethiprole was used as the internal standard (IS). The method was found to be linear over the range 5-500 ng/mL (r = 0.999). The limit of quantitation (LOQ) was validated at 5 ng/mL. The method was successfully applied to monitor plasma concentrations following subcutaneous administration of fipronil in cattle.
| Reference Key |
cid2012qumicadetermination
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|---|---|
| Authors | ;Yara P. Cid;Thais P. Ferreira;Deborah M. V. C. Medeiros;Rodrigo M. Oliveira;Nathália C. C. Silva;Viviane S. Magalhães;Fábio B. Scott |
| Journal | greece and rome |
| Year | 2012 |
| DOI |
10.1590/S0100-40422012001000029
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| URL | |
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