novel one-pot green synthesis of indolizines biocatalysed by candida antarctica lipases

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ID: 178223
2013
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Abstract
Marine microorganisms are of considerable interest as a promising source of enzymes with unsuspected potentials as catalysts for chemical synthesis. We describe here an efficient method for one-pot indolizine synthesis that has been developed using lipase A and lipase B from Candida antarctica as biocatalysts. As showed by HPLC/MS analysis, the yield in indolizines was higher in the presence of the biocatalyst than in absence of enzyme. Lipase A, from Candida antarctica, showed high catalytic activity and selectivity for the cycloaddition reactions. When the reactions were performed under ultrasound irradiation, the Candida antarctica lipase catalyzed reactions yielded pure indolozines, in good yields and in very short time.
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Authors ;Simon Bonte;Martine Demeunynck;Gabriela Bahrim;Ioana Otilia Ghinea;Bianca Furdui;Rodica Mihaela Dinica
Journal jixie gongcheng xuebao/journal of mechanical engineering
Year 2013
DOI
10.3390/md11020431
URL
http://www.mdpi.com/1660-3397/11/2/431
Keywords
cycloaddition

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