synthesis and characterization of oxovanadium (iv) dithiocarbamates with pyridine
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ID: 163693
2002
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Abstract
We report the synthesis and study of a new series of oxovanadium (IV) dithiocarbamate adducts and derivatives with pyridine and cyclohexyl, di-iso-butyl, di-n-propyl, anilin, morpholin, piperidin and di-iso-propyl amines. The complexes have been characterized by analytical, magnetochemical, IR, visible-UV spectral and thermal studies, and are assigned the formulas [VO(L)2].py, where L=cyclohexyl, di-iso-butyl, di-n-propyl, anilin dithiocarbamate and [VO(OH)(L)(py)2]OH.H2O (L=morpholin, piperidin and di-iso-propyl dithiocarbamate). The effect of the adduct formation on the pV=0 bound is discussed in terms of the IR (V=O, V-S and V-N stretching frequencies) and electronic spectra (d-d transitions).
| Reference Key |
doadrio2002qumicasynthesis
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| Authors | ;Antonio L. Doadrio;José Sotelo;Ana Fernández-Ruano |
| Journal | greece and rome |
| Year | 2002 |
| DOI |
10.1590/S0100-40422002000400002
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