(e)-3-(2,5-dimethoxyphenyl)-1-{[4-(2,5-dimethoxy-phenyl)-6-((e)-2,5-dimethoxystyryl)-2-thioxo-1,2,3,4-tetrahydropyrimidin-5-yl]}prop-2-en-1-one and (e)-3-(2,5-dimethoxyphenyl)-1-{[4-(2,5-dimethoxyphenyl)-6-methyl-2-thioxo-1,2,3,4-tetrahydropyrimidin-5-yl]}prop-2-en-1-one
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ID: 160069
2019
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Abstract
Dihydropyrimidine derivatives possess great potential to be used as a precursor for the synthesis of wide diverse dihydropyrimidine-like derivatives. In this research, the title compounds were synthesized through the reaction between 5-acetyl-4-(2,5-dimethoxyphenyl)-6-methyl-3,4-dihydropyrimidin-2(1H)-thione and 2,5-dimethoxybenzladehyde under aldol condensation condition. The title compound, (E)-3-(2,5-dimethoxyphenyl)-1-{[(4-(2,5-dimethoxyphenyl)-6-((E)-2,5-dimethoxystyryl)-2-thioxo-1,2,3,4-tetrahydropyrimidin-5-yl)]}prop-2-en-1-one (yield 15%), was obtained as major product, whereas (E)-3-(2,5-dimethoxyphenyl)-1-{[(4-(2,5-dimethoxyphenyl)-6-methyl-2-thioxo-1,2,3,4-tetrahydro pyrimidin-5-yl)]}prop-2-en-1-one (yield 8%) as side product through vinylogous aldol condensation.
| Reference Key |
suwito2019molbank(<i>e</i>)-3-(2,5-dimethoxyphenyl)-1-{[4-(2,5-dimethoxy-phenyl)-6-((<i>e</i>)-2,5-dimethoxystyryl)-2-thioxo-1,2,3,4-tetrahydropyrimidin-5-yl]}prop-2-en-1-one
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|---|---|
| Authors | ;Hery Suwito;Noorma Kurnyawaty;Ellyca Susetyo;Yuzkiya Azizah;Kautsar Ul Haq;Alfinda Novi Kristanti;Indriani Indriani |
| Journal | journal of chemical sciences |
| Year | 2019 |
| DOI |
10.3390/M1063
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| URL | |
| Keywords | Keywords not found |
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