application of vanadium incorporated phosphomolybdate supported on the modified kaolinin synthesis of diphenyl carbonate by oxidative carbonylation with phenol
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2017
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Abstract
Keggin-type molybdophosphoric acid, molybdophosphoric salt and vanadium incorporated molybdophosphoric salt supported on the modified kaolin (MK) were investigated as redox co-catalysts for the oxidative carbonylation of phenol to diphenyl carbonate (DPC) in the absence of solvent. The 20 wt.% of MnAMPV5 (one kind of vanadium incorporated molybdophosphoric salt) loaded on MK showed the highest catalytic activity with the yield of 24.68% and a TON of 306, while the selectivity amounts to nearly 100% in all the carbonylation reactions. The catalysts were characterized by XRD, BET, XPS and H2-TPR. The reusability study showed that the catalysts were stable and active.
| Reference Key |
meng2017chemicalapplication
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|---|---|
| Authors | ;Peng Meng;Yang Xiaojun;Wu Jiaxiong;Yuan Hua;Yin Chaofan;Wu Yuanxin |
| Journal | organon |
| Year | 2017 |
| DOI |
10.2298/CICEQ160701056P
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