addition of sedimentary rock to kaolinitic clays: influence on sintering process adição de rocha sedimentar às argilas cauliníticas: influência no processo de sinterização

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ID: 151604
2013
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Abstract
The physical and mechanical properties of clay-based ceramic probes with sedimentary rock added as the non-plastic component were evaluated. Samples were prepared with 0, 20, 40, 60 and 80 wt.% of rock added to the clay material. Pressed (7 ton) probes were sintered at 500, 800, 900, 1000, 1100 and 1200 °C and submitted to X-ray diffraction analysis and technological characterization. The X-ray diffraction results showed that the sedimentary rock had micaceous clay minerals, while the clay material had kaolinite as the main phases. Thermal analysis and X-ray diffraction showed reactions that indicated transformation (inversion of quartz), decomposition (loss of hydroxides) and phase formation (mullite) during heat treatment of the samples. The technological tests showed that the addition of sedimentary rock improved some properties of the sintered material, aided by the presence of fluxes. However, the presence of quartz in the rock hampered the formation of the mullite phase. The formation of new phases and transformations occurring during the heating and cooling of the samples helped explain the technological properties of ceramic materials.
Foram avaliadas, durante o processo de sinterização, as propriedades mecânicas de peças cerâmicas a base de argila com adição de rocha sedimentar. Foram preparados corpos de prova com 0, 20, 40, 60 e 80% em peso de rocha adicionada ao material argiloso. As peças foram sinterizadas nas temperaturas de 500, 800, 900, 1000, 1100 e 1200 °C e, posteriormente, submetidas à análise de difração de raios X e a ensaios tecnológicos Os resultados de difração de raios X mostram que a rocha sedimentar apresenta argilominerais micáceos enquanto o material argiloso possui a caulinita como fase principal. Técnicas de análises térmicas e difração de raios X das diferentes misturas mostram reações que indicam transformação (inversão do quartzo), decomposição (perda de hidróxidos) e formação de fase (mulita) durante o aquecimento das amostras. Os ensaios tecnológicos mostram que a adição da rocha sedimentar melhora algumas propriedades do material sinterizado, auxiliada pela presença de fundentes. Entretanto, a presença de quartzo na rocha dificulta a formação da fase mulita. A formação de novas fases e as transformações ocorridas no aquecimento e resfriamento das amostras ajuda explicar as propriedades tecnológicas dos materiais cerâmicos.
Reference Key
souza2013cermicaaddition Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors ;A. E. Souza;S. R. Teixeira;G. T. A. Santos;E. Longo
Journal Zootaxa
Year 2013
DOI
DOI not found
URL
http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132013000100017
Keywords
clay sintering fluxes civil engineering (general) mulliteengineering (general)

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