preparation and characterization of styrene bearing diethanolamine side group, styrene copolymer systems, and their metal complexes
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ID: 146963
2018
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Abstract
The two copolymer systems of styrene bearing diethanol amine side group and styrene were prepared by free radical polymerization method at 60°C in presence of 1,4-dioxane as solvent and AIBN as initiator. Their metal complexes were prepared by reaction of the copolymer used as ligand P(DEAMSt-co-St)L′′ and Ni(II) and Co(II) metal ions, which was carried out in presence of ethanol and NaOH at 65°C for 48 h in pH = 7.5. The structures of the copolymers used as ligand and metal complexes were identified by FT-IR, 1H-NMR spectra, and elemental analysis. The properties of the copolymers used as ligand and metal complexes were characterized by SEM-EDX, AAS, DSC, TGA, and DTA techniques. Then, the electrical properties of the copolymers and metal complexes were examined as a function of the temperature and frequency, and the activation energies (Ea) were estimated with conductivity measurements.
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akses2018internationalpreparation
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| Authors | ;Aslışah Açıkses;Necmittin Çömez;Fatih Biryan |
| Journal | 19th international congress of chemical and process engineering, chisa 2010 and 7th european congress of chemical engineering, ecce-7 |
| Year | 2018 |
| DOI |
10.1155/2018/6703783
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