2ii-vii, 3i-vii, 6i-vii-icosa-o-acetyl-2i-deoxy-cyclomaltoheptaose
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ID: 140617
2016
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Abstract
Deoxygenation of a secondary hydroxy group on β-cyclodextrin was conducted to prepare the title compound 2II-VII, 3I-VII, 6I-VII-icosa-O-acetyl-2I-deoxy-cyclomaltoheptaose. The synthetic procedure comprised a two-step reaction—phenoxythiocarbonylation and Barton-McCombie deoxygenation. The synthesized compound was characterized by 1H-NMR, 13C-NMR, HRMS, and elemental analysis.
| Reference Key |
miyagawa2016molbank2ii-vii,
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|---|---|
| Authors | ;Atsushi Miyagawa;Kazuki Kano;Aya Yoshida;Hatsuo Yamamura |
| Journal | journal of chemical sciences |
| Year | 2016 |
| DOI |
10.3390/M900
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