ω-methylsulfanylalkyl glucosinolates: a general synthetic pathway
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ID: 138991
2018
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Abstract
A general pathway was devised to synthesize ω-methylsulfanylalkyl glucosinolates, which represent an important class of structurally homogeneous plant secondary metabolites. The required thiofunctionalized hydroximoyl chlorides were obtained from the corresponding α,ω-nitroalkyl methylsulfide precursors, involving as the key-step, a nitronate chlorination strategy. A coupling reaction with 1-thio-beta-d-glucopyranose, followed by O-sulfation of the intermediate thiohydroximate and final deprotection of the sugar moiety afforded the target compounds.
| Reference Key |
mavratzotis2018molecules-methylsulfanylalkyl
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|---|---|
| Authors | ;Manolis Mavratzotis;Stéphanie Cassel;Sabine Montaut;Patrick Rollin |
| Journal | Journal of ethnopharmacology |
| Year | 2018 |
| DOI |
10.3390/molecules23040786
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| URL | |
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