on the reaction of 1,3-diphenylisobenzofuran and (2-iodoethynyl)(phenyl)iodonium triflate. a unique case of oxygen transfer from the diels-alder adduct to the diene
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2012
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Abstract
Reaction of 1,3-diphenylisobenzofuran (DPIBF) with 2-(iodoethynyl)(phenyl)-iodonium triflate at room temperature gave the expected Diels-Alder adduct, but using an excess of DFIBF (2 equiv.) and performing the reaction at 55 °C or heating at this temperature during the concentration stage, the initial orange solution or product mixture became dark brown and the products 1,2-phenylene-1,2-bis(phenylmethanone) and 2-(3-iodo-1,4-diphenylnaphthyl)(phenyl)iodonium triflate were obtained, which suggests an oxygen transfer between DPIBF and the initial adduct.
| Reference Key |
font-bardia2012moleculeson
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|---|---|
| Authors | ;Mercè Font-Bardia;Teresa Calvet;David Lozano;Pelayo Camps;Tània Gómez |
| Journal | Journal of ethnopharmacology |
| Year | 2012 |
| DOI |
10.3390/molecules17088795
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| URL | |
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