synthesis of 2-(9,10-dihydro-9,10-propanoanthracen-9-yl)-n-methylethanamine via a [4+2] cycloaddition
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ID: 129087
2010
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Abstract
The synthesis of the tetracyclic molecule 2-(9,10-dihydro-9,10-propano-anthracen-9-yl)-N-methylethanamine(2)as a homologue of the antidepressant 1-(9,10-dihydro-9,10-ethanoanthracen-9-yl)-N-methylmethaneamine (1) was described. The key intermediate 9-(prop-2-en-1-yl)-9,10-dihydro-9,10-propanoanthracen-12-one (7)was successfully synthesized via a [4+2] cycloaddition of α-bromoacrolein and 9-allyl-anthracene, followed by ring expansion and samarium diiodide deoxygenation.
| Reference Key |
karama2010moleculessynthesis
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|---|---|
| Authors | ;Usama Karama;Adel Al-Saidey;Zeid Al-Othman;Abdel Rahman Almansour |
| Journal | Journal of ethnopharmacology |
| Year | 2010 |
| DOI |
10.3390/molecules15064201
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| URL | |
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