electrochemical synthesis and spectroscopic characterization of poly(n-phenylpyrrole) coatings in an organic medium on iron and platinum electrodes
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ID: 128439
2008
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Abstract
The electrochemical synthesis of poly(N-phenylpyrrole) film was achieved on pretreated iron and platinum electrodes in acetonitrile solutions containing 0.1 M N-phenylpyrrole as the monomer and 0.1 M tetrabutylammonium trifluoromethane sulfonate (Bu4NCF3SO3) as the supporting-salt. The results showed that a surface treatment by 10 % aqueous nitric acid inhibits iron dissolution without preventing the N-phenylpyrrole oxidation. Very strongly adherent films were obtained at constant-potential, constant-current and cyclic voltammetry. XPS measurements, infrared (FT-IR) and electronic absorption (UV-vis) spectroscopies were used to characterize the iron and platinum-coated electrodes. Finally the anticorrosion properties of the PΦP film were evidenced.
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diaw2008bulletin<b>electrochemical
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| Authors | ;A.K.D. Diaw;D. Gningue-Sall;M. Fall;M.M. Dieng;J.J. Aaron |
| Journal | Experimental physiology |
| Year | 2008 |
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| Keywords | Keywords not found |
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