Solvent-controlled selective synthesis of biphenols and quinones via oxidative coupling of phenols.
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2017
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Abstract
A regioselective synthesis of unsymmetrical and symmetrical biphenols and binaphthols via oxidative coupling of phenols or naphthols in the presence of KSO in CFCOOH under ambient conditions is described. Interestingly, the 1ā:ā1 ratio of HO and CHCN solvent mixtures at 80 Ā°C instead of CFCOOH provided substituted unsymmetrical quinones. A gram-scale synthesis of biphenols and binaphthols was demonstrated.| Reference Key |
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| Authors | More, Nagnath Yadav;Jeganmohan, Masilamani; |
| Journal | Chemical communications (Cambridge, England) |
| Year | 2017 |
| DOI | 10.1039/c7cc04829g |
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