Crystal structure of '-[4-(di-methyl-amino)-benzyl-idene]furan-2-carbohydrazide monohydrate.
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ID: 107101
2020
The condensation of 2-furoic hydrazide and 4-dimethyl amino-benzaldehyde in ethanol yielded a yellow solid formulated as the title compound, CHNO·HO. The crystal packing is stabilized by inter-molecular O(water)-H⋯O,N(carbohydrazide) and N-H⋯O(water) hydrogen bonds, which form a two-dimensional network along the plane. Additional C-H⋯O inter-actions link the mol-ecules into a three-dimensional network. The dihedral angle between the mean planes of the benzene and the furan ring is 34.47 (6)°. The carbohydrazide moiety, , the C=N-N-C=O fragment and the benzene ring are almost coplanar, with an angle of 6.75 (9)° between their mean planes.
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syllagueye2020crystalacta
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| Authors | Sylla-Gueye, Rokhaya;Thiam, Ibrahima Elhadji;Orton, James;Coles, Simon;Gaye, Mohamed; |
| Journal | acta crystallographica section e, crystallographic communications |
| Year | 2020 |
| DOI | 10.1107/S205698902000465X |
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